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Judul Penentuan Sulfadiazin dengan Kromatografi Cair Kinerja Tinggi (HPLC)
Pengarang Unang Patriana
Ariestiana Permata Adji
EDISI Vol. 2, p. 47-49
Penerbitan Bogor BBPMSOH 1990
Deskripsi Fisik 3 tables; 4 ref. Summary (En)
Subjek Drugs -- PORK -- HPLC -- SULPHONAMIDES -- CALIBRATION
Catatan a High performance liquid chromatographic method (HPLC) for determination of sulfadiazine in swine meat was developed. Sulfadiazine was extracted from meat by homogenizing with acetonitrile. The homogenate was centrifuged and supermatant was evaporated. The extract was dissolved in 85% methanol and applied to an alumina coloumn. Sulfadiazine was eluted with acetonitrile-acetic acid water (22:1:78) and the eluate was applied to an HPLC coloumn packed with Nucleosil 5C18. The average recoveries of sulfadiazine added 1 ppm and 10 ppm to swine meat were 80.5% and 93.2%. The detection limit sulfadiazine by this method was 2.5ng.
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No Barcode No. Panggil Akses Lokasi Ketersediaan
Tag Ind1 Ind2 Isi
001 INLIS000000000000121
005 20210323091304
008 210323||||||||| | ||| |||| || |
035 0010-0321000121
041 $a en
100 0 $a Unang Patriana
245 0 0 $a Penentuan Sulfadiazin dengan Kromatografi Cair Kinerja Tinggi (HPLC)
250 $a Vol. 2, p. 47-49
260 $a Bogor $b BBPMSOH $c 1990
300 $a 3 tables; 4 ref. Summary (En)
500 $a a High performance liquid chromatographic method (HPLC) for determination of sulfadiazine in swine meat was developed. Sulfadiazine was extracted from meat by homogenizing with acetonitrile. The homogenate was centrifuged and supermatant was evaporated. The extract was dissolved in 85% methanol and applied to an alumina coloumn. Sulfadiazine was eluted with acetonitrile-acetic acid water (22:1:78) and the eluate was applied to an HPLC coloumn packed with Nucleosil 5C18. The average recoveries of sulfadiazine added 1 ppm and 10 ppm to swine meat were 80.5% and 93.2%. The detection limit sulfadiazine by this method was 2.5ng.
650 0 $a Drugs -- PORK -- HPLC -- SULPHONAMIDES -- CALIBRATION
700 0 $a Ariestiana Permata Adji
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