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Judul Penentuan residu antibiotik salinomisin, monensin dan lasalosid pada daging ayam dengan metoda bioautografi/kromatografi lapis tipis (TLC) dan kromatografi cair kinerja tinggi (HPLC)
Pengarang Syamsul Bahri Siregar
Sri Werdiningsih
Ni Made Ria Isriyanthi
Diana Hermawati
Fajar Sumping Catur Rasa
EDISI Vol. 4, p. 4-7
Penerbitan Bogor BBPMSOH 1995
Deskripsi Fisik 3 tables; 11 ref. Summary (En)
ISBN 0852-9612
Subjek Antibiotics -- Residues -- HPLC -- CHICKENS -- SALINOMYCIN -- MONENSIN -- LASALOCID -- THIN LAYER CHROMATOGRAPHY
Catatan A bioutography procedure was conducted to determine the risedue of salinomycin (SL), monensin (MN) and lasalosid (LS). SL, MN and LS were extracted from chicken meat by homogenizing with acetonitrile and purified by silica cartidge column. The aliquots were spotted on thin layer plate and detected by bioautography. Bacillus subtillis ATCC 6633 was used as test microorganisms. The percentage of averange recoveries of residues from chicken meat found at the level of SL 0.02 ppm, NM 0.05 ppm and LS 0.05 ppm were 73.90 ± 1.00%, 85.65 ± 2.17% and 76.26 ± 2.30%, respectively. A high performance liquid chromatography (HPLC) method with fluoremetric detector was used to determine the residue of LS in chicken meat. The method of extraction was conducted as decribe before. The aliquots were separated by HPLC using an ODS column. The percentage of average recoveries of LS at the level of 0.05 ppm was 75.71 ± 1.20% There was no differences between the percentage of averange recovery of LS at the level of 0.05 ppm wheathe
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No Barcode No. Panggil Akses Lokasi Ketersediaan
Tag Ind1 Ind2 Isi
001 INLIS000000000000110
005 20210323091301
008 210323||||||||| | ||| |||| || |
020 $a 0852-9612
035 0010-0321000110
041 $a id
100 0 $a Syamsul Bahri Siregar
245 0 0 $a Penentuan residu antibiotik salinomisin, monensin dan lasalosid pada daging ayam dengan metoda bioautografi/kromatografi lapis tipis (TLC) dan kromatografi cair kinerja tinggi (HPLC)
250 $a Vol. 4, p. 4-7
260 $a Bogor $b BBPMSOH $c 1995
300 $a 3 tables; 11 ref. Summary (En)
500 $a A bioutography procedure was conducted to determine the risedue of salinomycin (SL), monensin (MN) and lasalosid (LS). SL, MN and LS were extracted from chicken meat by homogenizing with acetonitrile and purified by silica cartidge column. The aliquots were spotted on thin layer plate and detected by bioautography. Bacillus subtillis ATCC 6633 was used as test microorganisms. The percentage of averange recoveries of residues from chicken meat found at the level of SL 0.02 ppm, NM 0.05 ppm and LS 0.05 ppm were 73.90 ± 1.00%, 85.65 ± 2.17% and 76.26 ± 2.30%, respectively. A high performance liquid chromatography (HPLC) method with fluoremetric detector was used to determine the residue of LS in chicken meat. The method of extraction was conducted as decribe before. The aliquots were separated by HPLC using an ODS column. The percentage of average recoveries of LS at the level of 0.05 ppm was 75.71 ± 1.20% There was no differences between the percentage of averange recovery of LS at the level of 0.05 ppm wheather using HPLC or LTC
650 0 $a Antibiotics -- Residues -- HPLC -- CHICKENS -- SALINOMYCIN -- MONENSIN -- LASALOCID -- THIN LAYER CHROMATOGRAPHY
700 0 $a Diana Hermawati
700 0 $a Fajar Sumping Catur Rasa
700 0 $a Ni Made Ria Isriyanthi
700 0 $a Sri Werdiningsih
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