Judul | Penentuan residu antibiotik salinomisin, monensin dan lasalosid pada daging ayam dengan metoda bioautografi/kromatografi lapis tipis (TLC) dan kromatografi cair kinerja tinggi (HPLC) |
Pengarang | Syamsul Bahri Siregar Sri Werdiningsih Ni Made Ria Isriyanthi Diana Hermawati Fajar Sumping Catur Rasa |
EDISI | Vol. 4, p. 4-7 |
Penerbitan | Bogor BBPMSOH 1995 |
Deskripsi Fisik | 3 tables; 11 ref. Summary (En) |
ISBN | 0852-9612 |
Subjek | Antibiotics -- Residues -- HPLC -- CHICKENS -- SALINOMYCIN -- MONENSIN -- LASALOCID -- THIN LAYER CHROMATOGRAPHY |
Catatan | A bioutography procedure was conducted to determine the risedue of salinomycin (SL), monensin (MN) and lasalosid (LS). SL, MN and LS were extracted from chicken meat by homogenizing with acetonitrile and purified by silica cartidge column. The aliquots were spotted on thin layer plate and detected by bioautography. Bacillus subtillis ATCC 6633 was used as test microorganisms. The percentage of averange recoveries of residues from chicken meat found at the level of SL 0.02 ppm, NM 0.05 ppm and LS 0.05 ppm were 73.90 ± 1.00%, 85.65 ± 2.17% and 76.26 ± 2.30%, respectively. A high performance liquid chromatography (HPLC) method with fluoremetric detector was used to determine the residue of LS in chicken meat. The method of extraction was conducted as decribe before. The aliquots were separated by HPLC using an ODS column. The percentage of average recoveries of LS at the level of 0.05 ppm was 75.71 ± 1.20% There was no differences between the percentage of averange recovery of LS at the level of 0.05 ppm wheathe |
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No Barcode | No. Panggil | Akses | Lokasi | Ketersediaan |
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Tag | Ind1 | Ind2 | Isi |
001 | INLIS000000000000110 | ||
005 | 20210323091301 | ||
008 | 210323||||||||| | ||| |||| || | | ||
020 | $a 0852-9612 | ||
035 | 0010-0321000110 | ||
041 | $a id | ||
100 | 0 | $a Syamsul Bahri Siregar | |
245 | 0 | 0 | $a Penentuan residu antibiotik salinomisin, monensin dan lasalosid pada daging ayam dengan metoda bioautografi/kromatografi lapis tipis (TLC) dan kromatografi cair kinerja tinggi (HPLC) |
250 | $a Vol. 4, p. 4-7 | ||
260 | $a Bogor $b BBPMSOH $c 1995 | ||
300 | $a 3 tables; 11 ref. Summary (En) | ||
500 | $a A bioutography procedure was conducted to determine the risedue of salinomycin (SL), monensin (MN) and lasalosid (LS). SL, MN and LS were extracted from chicken meat by homogenizing with acetonitrile and purified by silica cartidge column. The aliquots were spotted on thin layer plate and detected by bioautography. Bacillus subtillis ATCC 6633 was used as test microorganisms. The percentage of averange recoveries of residues from chicken meat found at the level of SL 0.02 ppm, NM 0.05 ppm and LS 0.05 ppm were 73.90 ± 1.00%, 85.65 ± 2.17% and 76.26 ± 2.30%, respectively. A high performance liquid chromatography (HPLC) method with fluoremetric detector was used to determine the residue of LS in chicken meat. The method of extraction was conducted as decribe before. The aliquots were separated by HPLC using an ODS column. The percentage of average recoveries of LS at the level of 0.05 ppm was 75.71 ± 1.20% There was no differences between the percentage of averange recovery of LS at the level of 0.05 ppm wheather using HPLC or LTC | ||
650 | 0 | $a Antibiotics -- Residues -- HPLC -- CHICKENS -- SALINOMYCIN -- MONENSIN -- LASALOCID -- THIN LAYER CHROMATOGRAPHY | |
700 | 0 | $a Diana Hermawati | |
700 | 0 | $a Fajar Sumping Catur Rasa | |
700 | 0 | $a Ni Made Ria Isriyanthi | |
700 | 0 | $a Sri Werdiningsih |
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