na INLIS000000000000110 20210323091301 210323||||||||| | ||| |||| || | 0852-9612 010-0321000110 id Syamsul Bahri Siregar Sri Werdiningsih Ni Made Ria Isriyanthi Diana Hermawati Fajar Sumping Catur Rasa Penentuan residu antibiotik salinomisin, monensin dan lasalosid pada daging ayam dengan metoda bioautografi/kromatografi lapis tipis (TLC) dan kromatografi cair kinerja tinggi (HPLC) Vol. 4, p. 4-7 Bogor BBPMSOH 1995 3 tables; 11 ref. Summary (En) A bioutography procedure was conducted to determine the risedue of salinomycin (SL), monensin (MN) and lasalosid (LS). SL, MN and LS were extracted from chicken meat by homogenizing with acetonitrile and purified by silica cartidge column. The aliquots were spotted on thin layer plate and detected by bioautography. Bacillus subtillis ATCC 6633 was used as test microorganisms. The percentage of averange recoveries of residues from chicken meat found at the level of SL 0.02 ppm, NM 0.05 ppm and LS 0.05 ppm were 73.90 ± 1.00%, 85.65 ± 2.17% and 76.26 ± 2.30%, respectively. A high performance liquid chromatography (HPLC) method with fluoremetric detector was used to determine the residue of LS in chicken meat. The method of extraction was conducted as decribe before. The aliquots were separated by HPLC using an ODS column. The percentage of average recoveries of LS at the level of 0.05 ppm was 75.71 ± 1.20% There was no differences between the percentage of averange recovery of LS at the level of 0.05 ppm wheather using HPLC or LTC Antibiotics -- Residues -- HPLC -- CHICKENS -- SALINOMYCIN -- MONENSIN -- LASALOCID -- THIN LAYER CHROMATOGRAPHY